[Application of two-color infrared fluorescence for detection of protein phosphorylation]

Nan Fang Yi Ke Da Xue Xue Bao. 2006 Feb;26(2):150-3.
[Article in Chinese]

Abstract

Objective: To assess the value of two-color infrared fluorescence imaging system in detecting protein phosphorylation in comparison with chemiluminescent detection.

Method: The lung tissue homogenate of mice treated with lipopolysaccharide (LPS) for different time lengths were prepared to separate the proteins by SDS-polyacrylamide gel electrophoresis followed by transfer of the proteins onto PVDF membranes. The membranes were incubated with the antibodies against total p42/44 MAPK/phospho-p42/44 MAPK, and then with goat anti-mouse or anti-rabbit secondary antibodies conjugated to Alexa Fluor 680, IRDye 800 or horseradish peroxidase. The blotted proteins were detected and quantified using Odyssey infrared imaging system or chemiluminescent detection.

Results: LPS treatment rapidly induced p42/44 MAPK phosphorylation, which reached the peak level 1 h after the treatment and resumed the baseline level at 12 h. Consistent results were obtained by the two detection methods, but two-color infrared fluorescence imaging system showed better sensitivity in detecting the target protein, and was easy to manipulate with good efficiency and capable of analyzing two proteins simultaneously.

Conclusion: Two-color infrared fluorescence system is a powerful system for detecting phosphorylation of proteins.

Publication types

  • English Abstract
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Blotting, Western / instrumentation
  • Blotting, Western / methods*
  • Fluorescence
  • Fluorescent Dyes / chemistry
  • Lipopolysaccharides
  • Luminescent Measurements / instrumentation
  • Luminescent Measurements / methods
  • Lung / drug effects
  • Lung / enzymology
  • Lung / pathology
  • Mice
  • Mice, Inbred BALB C
  • Mitogen-Activated Protein Kinase 1 / chemistry
  • Mitogen-Activated Protein Kinase 1 / metabolism*
  • Mitogen-Activated Protein Kinase 3 / chemistry
  • Mitogen-Activated Protein Kinase 3 / metabolism*
  • Phosphorylation
  • Reproducibility of Results
  • Shock, Septic / chemically induced
  • Shock, Septic / enzymology

Substances

  • Fluorescent Dyes
  • Lipopolysaccharides
  • Mitogen-Activated Protein Kinase 1
  • Mitogen-Activated Protein Kinase 3