Synthesis of peptides as cloned ubiquitin extensions

J Biol Chem. 1989 Oct 15;264(29):17078-83.

Abstract

Oligonucleotides encoding four peptides ranging in length from 10 to 21 amino acids were cloned between the Afl2 and KpnI sites in the ubiquitin expression vector, pNMHUb. Escherichia coli AR13, a strain that contains a temperature-sensitive lambda repressor, was transformed by the plasmids, and upon shift to 42 degrees C, the cells produced large amounts of ubiquitin extended at its carboxyl terminus by each of the four peptides. Following a simple three-step purification of the ubiquitin fusion proteins, the peptides were cleaved from ubiquitin using a ubiquitin-alpha-protein hydrolase isolated from rabbit reticulocytes. The released ubiquitin molecules were shown to be competent in conjugation assays, and amino acid analyses of the purified peptides revealed that full length products were obtained in all cases. Since peptide yields varied from 2 to 4 mg/liter of culture medium, ubiquitin extensions provide an attractive alternative to solid phase synthesis for the production of peptides.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Amino Acids / analysis
  • Animals
  • Cloning, Molecular*
  • DNA Restriction Enzymes
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Gene Expression
  • Molecular Sequence Data
  • Oligonucleotides / genetics
  • Peptide Biosynthesis*
  • Peptides / genetics
  • Peptides / isolation & purification
  • Plasmids
  • Rabbits
  • Recombinant Fusion Proteins / genetics
  • Reticulocytes / enzymology
  • Transformation, Bacterial
  • Ubiquitins / biosynthesis*
  • Ubiquitins / genetics

Substances

  • Amino Acids
  • Oligonucleotides
  • Peptides
  • Recombinant Fusion Proteins
  • Ubiquitins
  • DNA Restriction Enzymes