Enantiodivergent Synthesis of 1-Heteroaryl Tetrahydroisoquinolines Catalyzed by Imine Reductases

Org Lett. 2023 Apr 14;25(14):2438-2443. doi: 10.1021/acs.orglett.3c00603. Epub 2023 Apr 3.

Abstract

Two enantiocomplementary imine reductases (IREDs) with high enantioselectivity were identified with catalytic activity toward the reduction of 1-heteroaryl dihydroisoquinolines through a screening of wild-type IREDs and enzyme engineering. Furthermore, (R)-IR141-L172M/Y267F and (S)-IR40 were applied to access a series of different 1-heteroaryl tetrahydroisoquinolines with high to excellent ee values (82 to >99%) and isolated yields (80 to 94%), thereby providing an effective method to construct this class of pharmaceutically important alkaloids, such as the intermediate of kinase inhibitor TAK-981.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biocatalysis
  • Imines
  • Oxidoreductases* / metabolism
  • Stereoisomerism
  • Tetrahydroisoquinolines*

Substances

  • Imines
  • Oxidoreductases
  • Tetrahydroisoquinolines